ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

更新時(shí)間：2021-01-12

簡要描述：

ACQUITY UPLC方法驗(yàn)證系統(tǒng)包
提供三批色譜填料（來自不同批次的顆?；w）以判斷一個(gè)分析方法的耐受性，可靠性和一致性。

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ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

UPLC方法驗(yàn)證包— 確保方法耐用性

為了確保分析方法持續(xù)可靠且具有重現(xiàn)性，采用多批色譜填料進(jìn)行檢測(cè)和驗(yàn)證變得尤為重要。作為硅膠雜化顆粒的主要生產(chǎn)商，沃特世公司為不同批次之間的重現(xiàn)性設(shè)立了行業(yè)的基準(zhǔn)?；谛抛u(yù)*的顆粒和色譜柱生產(chǎn)的過程控制，使批與批和柱與柱之間的變異性小化，從而為分析方法長期的可靠性提供信心。

ACQUITY UPLC方法驗(yàn)證包提供三批色譜填料(來自不同批次的顆粒基體)以判斷一個(gè)分析方法的耐受性，可靠性和一致性。

來自三個(gè)不同批次的填料基體的三個(gè)不同批次的鍵合處理的ACQUITY UPLC柱對(duì)氯氨平有關(guān)物質(zhì)的分析表現(xiàn)出zhuo越的重現(xiàn)性，保證了分析方法的長期重現(xiàn)性。

選擇性(a)
批號(hào)	雜質(zhì)C	雜質(zhì)A	氯氨平	雜質(zhì)B
119	1.03	1.07	1.07	1.59
120	1.03	1.07	1.07	1.58
124	1.02	1.07	1.07	1.58

ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

訂貨信息：

ACQUITY UPLC方法開發(fā)套裝[MDK: Method Development Kit]

套裝名稱	數(shù)量	固定相	顆粒大小	配置	部件編號(hào)
選擇性大化大化UPLC方法開發(fā)套裝：寬泛的選擇性用于方法開發(fā)，包括在低pH和高pH下。是低離子強(qiáng)度添加劑條件時(shí)(例如甲酸)的佳佳選擇
選擇性*大化UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB	CSH 1.7 μm; HSS 1.8 μm	2.1 x 50 mm	176002123
選擇性*大化UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB	CSH 1.7 μm; HSS 1.8 μm	2.1 x 100 mm	176002124
選擇性*大化UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB	CSH 1.7 μm; HSS 1.8 μm	3.0 x 50 mm	176002125
選擇性*大化UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SB	CSH 1.7 μm; HSS 1.8 μm	3.0 x 100 mm	176002126
高&低pH，寬選擇性的UPLC色譜柱套裝：通過開拓低和高流動(dòng)相pH使分離選擇性寬
高&低pH，寬選擇性的UPLC色譜柱套裝	4件/包	BEH C18, BEH C8, BEH Shield RP18, BEH苯基	BEH 1.7 μm	2.1 x 50 mm	176001042
高&低pH，寬選擇性的UPLC色譜柱套裝	4件/包	BEH C18, BEH C8, BEH Shield RP18, BEH苯基	BEH 1.7 μm	2.1 x 100 mm	176001043
高&低pH，寬選擇性的UPLC色譜柱套裝	4件/包	BEH C18, BEH C8, BEH Shield RP18, BEH苯基	BEH 1.7 μm	3.0 x 50 mm	176001881
高&低pH，寬選擇性的UPLC色譜柱套裝	4件/包	BEH C18, BEH C8, BEH Shield RP18, BEH苯基	BEH 1.7 μm	3.0 x 100 mm	176001882
UPLC方法開發(fā)套裝：通過開拓低和高流動(dòng)相pH(BEH色譜柱)將分離選擇性*大化大化和適用于極性化合物保留性(HSS T3)
UPLC方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH 苯基, HSS T3	BEH 1.7 μm; HSS 1.8 μm	2.1 x 50 mm	176001603
UPLC方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH 苯基, HSS T3	BEH 1.7 μm; HSS 1.8 μm	2.1 x 100 mm	176001604
UPLC方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH 苯基, HSS T3	BEH 1.7 μm; HSS 1.8 μm	3.0 x 50 mm	176001883
UPLC方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH 苯基, HSS T3	BEH 1.7 μm; HSS 1.8 μm	3.0 x 100 mm	176001884
L1 UPLC色譜柱套裝：依從USP藥典中L1類別，但提供不同硅醇基活性和疏水性的C18色譜柱
L1 UPLC色譜柱套裝	4件/包	BEH C18, BEH Shield RP18, HSS C18, HSS T3	BEH 1.7 μm; HSS 1.8 μm	2.1 x 50 mm	176001605
L1 UPLC色譜柱套裝	4件/包	BEH C18, BEH Shield RP18, HSS C18, HSS T3	BEH 1.7 μm; HSS 1.8 μm	2.1 x 100 mm	176001606
L1 UPLC色譜柱套裝	4件/包	BEH C18, BEH Shield RP18, HSS C18, HSS T3	BEH 1.7 μm; HSS 1.8 μm	3.0 x 50 mm	176001885
L1 UPLC色譜柱套裝	4件/包	BEH C18, BEH Shield RP18, HSS C18, HSS T3	BEH 1.7 μm; HSS 1.8 μm	3.0 x 100 mm	176001886
質(zhì)譜UPLC色譜柱套裝：直鏈烷烴C18柱，具有不同的硅醇活性、峰形、選擇性和疏水性，且無MS流失問題
質(zhì)譜UPLC色譜柱套裝	4件/包	BEH C18, HSS C18, HSS T3, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	2.1 x 50 mm	176001607
質(zhì)譜UPLC色譜柱套裝	4件/包	BEH C18, HSS C18, HSS T3, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	2.1 x 100 mm	176001608
質(zhì)譜UPLC色譜柱套裝	4件/包	BEH C18, HSS C18, HSS T3, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	3.0 x 50 mm	176001887
質(zhì)譜UPLC色譜柱套裝	4件/包	BEH C18, HSS C18, HSS T3, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	3.0 x 100 mm	176001888
低pH，寬選擇性UPLC色譜柱套裝：有各種不同的鍵合相和選擇性，用于開發(fā)低pH流動(dòng)相條件下的反相方法
低pH，寬選擇性UPLC色譜柱套裝	4件/包	BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	2.1 x 50 mm	176001609
低pH，寬選擇性UPLC色譜柱套裝	4件/包	BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	2.1 x 100 mm	176001610
低pH，寬選擇性UPLC色譜柱套裝	4件/包	BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	3.0 x 50 mm	176001889
低pH，寬選擇性UPLC色譜柱套裝	4件/包	BEH Shield RP18, BEH 苯基, HSS C18, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	3.0 x 100 mm	176001890
選擇性*大化大化的RP 和 HILIC UPLC方法開發(fā)套裝：通過綜合HILIC和RP固定相以提供寬分離選擇性，用以保留分離跨越寬泛極性范圍的分析物
選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, BEH Amide	CSH 1.7 μm; BEH 1.7 μm	2.1 x 50 mm	176002127
選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, BEH Amide	CSH 1.7 μm; BEH 1.7 μm	2.1 x 100 mm	176002128
選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, BEH Amide	CSH 1.7 μm; BEH 1.7 μm	3.0 x 50 mm	176002129
選擇性*大化的RP 和 HILIC UPLC方法開發(fā)套裝	4件/包	CSH C18, CSH苯己基, CSH氟苯基, BEH Amide	CSH 1.7 μm; BEH 1.7 μm	3.0 x 100 mm	176002130
UPLC RP和HILIC方法開發(fā)套裝：通過綜合RP和HILIC固定相以提供寬分離選擇性，用以保留分離跨越寬泛極性范圍的分析物
UPLC RP和HILIC 方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	2.1 x 50 mm	176001959
UPLC RP和HILIC 方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	2.1 x 100 mm	176001960
UPLC RP和HILIC 方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	3.0 x 50 mm	176001961
UPLC RP和HILIC 方法開發(fā)套裝	4件/包	BEH C18, BEH Shield RP18, BEH Amide, HSS C18 SB	BEH 1.7 μm; HSS 1.8 μm	3.0 x 100 mm	176001962
UPLCHILIC方法開發(fā)套裝：在低pH(對(duì)堿性分析物)和高pH(對(duì)酸性分析物)下為極性和/或可離子化化合物輕松開發(fā)HILIC方法
UPLCHILIC方法開發(fā)套裝	4件/包	BEH Amide, BEH HILIC	BEH 1.7 μm	2.1 x 50 mm	176001963
UPLCHILIC方法開發(fā)套裝	4件/包	BEH Amide, BEH HILIC	BEH 1.7 μm	2.1 x 100 mm	176001964
UPLCHILIC方法開發(fā)套裝	4件/包	BEH Amide, BEH HILIC	BEH 1.7 μm	3.0 x 50 mm	176001965
UPLCHILIC方法開發(fā)套裝	4件/包	BEH Amide, BEH HILIC	BEH 1.7 μm	3.0 x 100 mm	176001966

ACQUITY UPLC方法轉(zhuǎn)換套裝[MTK: Method Transfer Kit]*

套裝名稱	UPLC Column 2.1 mm ID	HPLC Column 4.6 mm ID	部件編號(hào)
CSH C18 1.7 to 5 μm MTK	50 mm, 1.7 μm	150 mm, 5 μm	186005529
CSH Phenyl-Hexyl 1.7 to 5 μm MTK	50 mm, 1.7 μm	150 mm, 5 μm	186005530
CSH Fluoro-Phenyl 1.7 to 5 μm MTK	50 mm, 1.7 μm	150 mm, 5 μm	186005531
BEH C18 1.7 to 5 μm MTK	50 mm, 1.7 μm	150 mm, 5 μm	186004958
BEH Shield RP18 1.7 to 5 μm MTK	50 mm, 1.7 μm	150 mm, 5 μm	186004959
BEH HILIC 1.7 to 5 μm MTK	50 mm, 1.7 μm	150 mm, 5 μm	186004960
HSS C18 1.8 to 5 μm MTK	50 mm, 1.8 μm	150 mm, 5 μm	186004961
HSS T3 1.8 to 5 μm MTK	50 mm, 1.8 μm	150 mm, 5 μm	186004962
HSS C18 SB 1.8 to 5 μm MTK	50 mm, 1.8 μm	150 mm, 5 μm	186004963
HSS Cya.8 to 5 μm MTK	50 mm, 1.8 μm	150 mm, 5 μm	186005979
HSS PFP 1.8 to 5 μm MTK	50 mm, 1.8 μm	150 mm, 5 μm	186006000
CSH C18 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186005532
CSH Phenyl-Hexyl 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186005533
CSH Fluoro-Phenyl 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186005534
BEH C18 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186004964
BEH Shield RP18 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186004965
BEH HILIC 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186004966
BEH Amide 1.7 to 3.5 μm MTK	50 mm, 1.7 μm	100 mm, 3.5 μm	186004967
HSS C18 1.8 to 3.5 μm MTK	50 mm, 1.8 μm	100 mm, 3.5 μm	186004968
HSS T3 1.8 to 3.5 μm MTK	50 mm, 1.8 μm	100 mm, 3.5 μm	186004969
HSS C18 SB 1.8 to 3.5 μm MTK	50 mm, 1.8 μm	100 mm, 3.5 μm	186004970
HSS Cya.8 to 3.5 μm MTK	50 mm, 1.8 μm	100 mm, 3.5 μm	186005980
HSS PFP 1.8 to 3.5 μm MTK	50 mm, 1.8 μm	100 mm, 3.5 μm	186006001
CSH C18 1.7 to 3.5 μm High Rs MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186005535
CSH Phenyl-Hexyl 1.7 to 3.5 μm高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186005536
CSH Fluoro-Phenyl 1.7 to 3.5 μm高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186005537
BEH C18 1.7 to 3.5 μm 高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004971
BEH Shield RP18 1.7 to 3.5 μm高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004972
BEH HILIC 1.7 to 3.5 μm 高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004973
BEH Amide 1.7 to 3.5 μm 高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004974
HSS C18 1.8 to 3.5 μm 高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004975
HSS T3 1.8 to 3.5 μm 高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004976
HSS C18 SB 1.8 to 3.5 μm 高分辨 MTK	100 mm, 1.7 μm	150 mm, 3.5 μm	186004977
HSS Cya.8 to 3.5 μm 高分辨 MTK	100 mm, 1.8 μm	150 mm, 3.5 μm	186005981
HSS PFP 1.8 to 3.5 μm 高分辨 MTK	100 mm, 1.8 μm	150 mm, 3.5 μm	186006002

*每個(gè)套裝都含有一根UPLC色譜柱和一根HPLC色譜柱，可從ACQUITY UPLC在線社區(qū)
www.waters。。ｃｏｍ/myuplc下載ACQUITY UPLC Columns Calculator用于計(jì)算方法轉(zhuǎn)移。

ACQUITY UPLC方法驗(yàn)證套裝[MVK:Method Validation Kit]**

固定相	粒徑	色譜柱長度	部件編號(hào) 2.1 mm ID	部件編號(hào) 3.0 mm ID
CSH C18	1.7 μm	50 mm	186005571	186005573
CSH C18	1.7 μm	100 mm	186005572	186005574
CSH 苯己基	1.7 μm	50 mm	186005579	186005581
CSH 苯己基	1.7 μm	100 mm	186005580	186005582
CSH 氟苯基	1.7 μm	50 mm	186005575	186005577
CSH 氟苯基	1.7 μm	100 mm	186005576	186005578
BEH C18	1.7 μm	50 mm	186004044	186004691
BEH C18	1.7 μm	100 mm	186004045	186004692
BEH C8	1.7 μm	50 mm	186004046	186004693
BEH C8	1.7 μm	100 mm	186004047	186004694
BEH Shield RP18	1.7 μm	50 mm	186004048	186004695
BEH Shield RP18	1.7 μm	100 mm	186004049	186004696
BEH Phenyl	1.7 μm	50 mm	186004050	186004697
BEH Phenyl	1.7 μm	100 mm	186004052	186004698
BEH HILIC	1.7 μm	50 mm	186004053	186004699
BEH HILIC	1.7 μm	100 mm	186004054	186004700
BEH Amide	1.7 μm	50 mm	186004807	186004809
BEH Amide	1.7 μm	100 mm	186004808	186004810
BEH130 C18	1.7 μm	100 mm	186004896	-
BEH300 C18	1.7 μm	100 mm	186004897	-
BEH300 C4	1.7 μm	100 mm	186004899	-
寡核苷酸 C18	1.7 μm	100 mm	186004898	-
Glycan BEH Amide	1.7 μm	100 mm	186004907	-
HSS T3	1.8 μm	50 mm	186004055	186004701
HSS T3	1.8 μm	100 mm	186004056	186004702
HSS C18	1.8 μm	50 mm	186004057	186004703
HSS C18	1.8 μm	100 mm	186004058	186004704
HSS C 18 SB	1.8 μm	50 mm	186004137	186004705
HSS C 18 SB	1.8 μm	100 mm	186004138	186004709
HSS PFP	1.8 μm	50 mm	186005975	-
HSS PFP	1.8 μm	100 mm	186005976	-
HSS PFP	1.8 μm	50 mm	186005977	-
HSS PFP	1.8 μm	100 mm	186005978	-
HSS 氰基	1.8 μm	50 mm	186005996	186005998
HSS 氰基	1.8 μm	100 mm	186005997	186005999

**每個(gè)套裝包括來自3個(gè)不同批次填料的3根色譜柱。

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ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

ACQUITY UPLC方法驗(yàn)證系統(tǒng)包

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